The department hosts state of the art facilities to conduct solid/ liquid/ gas phase analysis for guiding fundamental and applied chemical engineering research. The Analytical Laboratory of the department houses sophisticated instruments having a wide variety of applications like Particle Characterization, Concentration Measurement, Titration, Rheological property analysis etc.

Facilities Available in Analytical Laboratory:
Instruments available for analysis and their typical applications are given below:

Sl No Name of Instruments Status Remarks
1. Atomic Absorption Spectrophotometer (AAS) Working  
2. Autotitrator Not Working Burrete is not working
3. BET Surface Area Analyzer Working  
4. Chemisorb Working  
5. Differential Scanning Calorimetry  (DSC) Working  
6. Delsa Nano Working  
7. FTIR Working  
8. Gas Chromatograph (GC) Working  
9. Gas Chromatography-Mass Spectrometer (GC-MS) Working  
10. High Performance Liquid Chromatograph (HPLC) (PerkinElmer) Working  
11. High Performance Liquid Chromatograph (Shimadzu) Working  
12. Karl Fischer Titrator Working  
13. Laser Particle Size Analyzer (LPSA) Not Working Engineer will visit soon
14. Lyophilizer Working  
15. Millipore Water Synthesis Unit Working  
16. Polarimeter Working  
17. Rheometer Working  
18. Rotavapor Working  
19. Spining Drop Tensiometer Working  
20. Tensiometer Working  
21. Thermo Gravimetric Analyzer Working  
22. TOC-Analyzer Working  
23. UV Vis Spectrophotometer(PerkinElmer) Working  
24. UV Visible Spectrophotometer ( Shimadzu) Working  
DST- FIST Funded Analytical Instruments:
Sl No Name of Instrument Status Remarks
25. Working  
26. Working  
27. Working  
28.
 XRD
Not Working  
Auxiliary Instruments
Sl No Name of Instrument Status Remarks
1. Centrifuge (Model No. :2-16P,  Make: Sigma, Germany) Working  
2.
Chillers (Model No. : F32, Make:  Julabo,Germany)
Working  
3.
Chillers (Model No. : TC 45, Make: Huber USA)
Working  
4. Digital Balance ( Model No.: ME204, Make: Mettler Toledo, Switzerland) Working  
5. Circulating Baths (Model No. : RW-2025G, Make: Lab Companion, USA) Working  
6. Conductivity Meter (Model No. :  51E, Make: Electronics, India Working  
7. Dehumidifier (Model No. : - Oº , Make: - Origin: - Mumbai) Working  
8. Digital Balance (Model No. : ME 204, Make: Mettler Toledo, Switzerland) Working  
9. High Resolution Microscope (Model No. : Axiostar plus, Make: Carl Zeiss, Germany) Working  
10. pH Meter (Model No. : pH 700; Make: Eutech Instruments, Singapore) Working  
11. Polarimeter ( Model No.:  14-8.5-100-6.0, Make: Rudolph, USA)      Working  
12. Rotavapr ( Model No.: R 300, Make: Buchi, Switzerland) Working  
13. Sonicator ( Model No.: 3.5 L/00H/DTC, Make: PCi, Mumbai) Working  
 
In charge of the Lab Lab Address
Dr. Vaibhav V. Goud
Associate Professor
Department of Chemical Engineering
Indian Institute of  Technology Guwahati
E-mail    : vvgoud@iitg.ac.in
Phone    : +91 361 2582272
Fax        : +91 361 2582291
Location : Room No: 005
Analytical Lab
Department of Chemical Engineering
Indian Institute of  Technology Guwahati
Email              : analyticallab@iitg.ernet.in
Phone             : +91 361 258 2294
Location          : Analytical Laboratory, 1st Floor.
   

The instruments in the Analytical Laboratory are available for analysis to other Departments and Centers within IITG as well as other Institutes and External Agencies.
To request an analysis with any of our instruments:

Internal User (from IIT Guwahati) : Is required to register his/ her request through an Analysis Request form. Click here to download Analysis Request form.
External User (outside IIT Guwahati): For requesting Analysis, please Click here
Please Contact: HoD Chemical Engineering: 03612582251 or 
Chemical Engineering Office -0361 2582300/ Analytical Lab -0361 2582294.

Instruments

1. Atomic Absorption Spectrophotometer (AAS)
(Model No.: Spectra AA 220 FS; Make: M/s Varian, Netherland)
Use to determine metal ion concentration using flame mode. Uses air-acetylene or nitrous oxide- acetylene burner. Equipped with vapor generation accessory and electro thermal controller for flameless hydride vapor analysis.


 



2. Auto Titrator
(Model No.: DL-50; Make: M/s Mettler Toledo, Switzerland)

Concentration determination with highest precision and productivity.



3. BET Surface Area Analyzer 
(Model No.: Tristar II; Make: M/s Micromeritics, U.S.A.)
For measuring the surface area and pore size distribution measurement at liquid nitrogen temperature. Important instrument in particle characterization.



4. Chemisorb

(Model No.: Chemisorb 2720; Make: M/s Micromeritics , USA)
Use to measure the percent dispersion, active metal area, Crystallite & quantify acid or base site using pulse chemisorb.



5. Differential Scanning Calorimetry (DSC)
(Model No.: DSC 1; Make: M/s Mettler Toledo, Switzerland)
Differential scanning calorimetry can be used to measure a number of characteristic properties of a sample. Using this technique it is possible to observe fusion and crystallization events as well as glass transition temperatures TG   


6. Delsa Nano
(Model No.: Delsa Nano C; Make: M/s Beckman Coulter, Swtizerland)

Used to measure to Zeta Potential/ Submicron size analysis (0.6 nm to 7.0 Micron) with forward 15 Deg & backscatter 165 Deg.

 


7. Fourier Transform Infra-Red Spectroscopy (FTIR)
(Model No.: IRAffinity-1; Make: M/s Shimadzu, Japan)

FTIR can be used for identification of functional group in raw material, polymeric films & Qualitative analysis. Use for powdered & liquid samples


8. Gas Chromatograph (GC)
(Model No.: CP-3800; Make: M/s Varian, Netherland)

For typical gas chromatography applications with provision for gas as well as liquid injection of samples. Equipped with three detectors viz. TCD (Thermal conductivity detector), ECD (electron capture detector) and FID (Flame ionization detector).

 


9. Gas Chromatography-Mass Spectrometer (GC-MS)
(Model No.: 450-GC, 240-MS; Make: M/s Varian, Netherland)

Gas-liquid chromatography and mass spectrometry to identify different substances within a test sample. Applications of GC-MS include drug detection, fire investigation, explosives investigation, and identification of unknown samples.

 


10. High Performance Liquid Chromatograph (HPLC)
(Model No.: Series200; Make: M/s PerkinElmer, Switzerland)

HPLC system for chromatographic separations. Equipped with RI and UV-Visible detectors.
 
 
 


11. High Performance Liquid Chromatograph (HPLC)
(Model No.: Prominence HPLC System; Make: M/s Shimadzu, Singapore)
HPLC system for chromatographic separations. Equipped with RI and UV-Visible detectors
 


12. Karl Fischer Titrator
(Model No.: 878 KF; Make: M/s Metrohm, Switzerland)
Use to determine the moisture content of the sample. Uses pyridine free Karl Fischer reagent for titration and dry methanol as solvent.


13. Laser Particle Size Analyzer (LPSA)

(Model No.: Master sizer 2000; Make: M/s Malvern, UK)
Measures particle size distribution of suitably dispersed field of particles in the range 0.02 to 2000 micron. Provision for both dry (using air as dispersing media) and wet (using suitable dispersant) Dispersion available.


14. Lyophilizer
(Model No.: Alpha 2-4 LD; Make: M/s Martin Christ, Germany)
Equipment is solely designed for freeze drying of solid or liquid products in ampoules, vials or Dishes
 


15. Millipore Water Synthesis Unit
(Model No.: Elix-3, Milli-Q; Make: M/s Millipore, USA)

Used for synthesis of de-ionized water applying RO and EDI technology. Synthesizing grade-1 water with resistivity -18.2 megaohms.cm, TOC <10ppb and particle <1 (0.22micorns per ml) indispensable for various experimental, reaction and analytical purposes


 


16. Rheometer
(Model No.: Rheostress RS 1; Make: M/s Thermo Electron, Germany)
Used for dedicated study of rheological properties of fluids, both Newtonian and Non-Newtonian. Equipped with several measurement geometries like cone-plate, cone-cup, and serrated Cone etc.


17. Spinning Drop Tensiometer
(Model No.: SITE 100; Make: M/s KRUSS gmbH, Germany)

Used to Measure the interfacial tension between two liquids & analyzing video image of a drop in a Rotating capillary upto 10-6 mN/m.


 


18. Tensiometer
(Model No.: DY300; Make: M/s Kwoya, Japan)

Instrument dedicated to the study of sruface tension & interfacial tenaion Using ring & plate method.  


19. Thermo Gravimetric Analyzer
(TGA)
(Model No.: TG 209 F1 Libra; Make: M/s Netzsch, Germany)
For differential thermo gravimetric studies, SDTA analyses under defined atmosphere (inert or reactive). With temperature programming up to 40 segment runs, furnace temperature up to 11000C and  measurement precision up to 1 microgram.


20. TOC-Analyzer
(Model No.: Aurora 1030 C; Make: M/s O.I. Analytical, USA)     
TOC analyzer is totally automatic system for analyzing aqueous samples for Total Organic Carbon (TOC) and Total Inorganic Carbon (TIC). Using heated per-sulfate oxidation technology, samples containing 2 ppb to 30,000 ppm of organic carbonate analyzed. 



21. UV Vis Spectrophotometer
(Model No.: Lambda 35; Make: M/s PerkinElmer, Switzerland)
Use to determine the absorption/ transmission spectra of the analyte. Different measurement methods like concentration, wave program and time drive method available. Typical application includes concentration measurement.



22. UV Vis Spectrophotometer
(Model No.: UV-2600, Make: Shimadzu, Singapore)
UV-2600 can be used for measurement of solar cell Anti-reflective films and polycrystalline silicon wafers.

DST-FIST Funded Analytical Instruments:


1. Ellipsometer:
(Model No.: Nanofilm_ep3sw, Make: Accurion GmbH, Germany)
To measure optical constant, thickness and refractive index of thin film. Also equipped with Langmuir-Blodgett troughs to prepare more layer films.
 
 

2. Gas Chromatograph:
(Model No.: 450-GC, Make: Bruker, Germany)
For typical gas chromatography applications. Equipped with three detectors viz. TCD (thermal conductivity detector), Pulse Flame photometric Detector) and FID (Flame ionization detector).
 


3. Interfacial Rheometer:
(Model No.: Physica MCR 301, Make: Anton Paar, Austria)
Rheological measurements of interfacial films at gas/liquid and liquid/liquid interfaces.
 


4. XRD:
(Model No.: D8 Advance, Make: Bruker, Netherlands)
Powder X-ray diffraction application used for structure determination, crystallinity and phase identification.